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20 SCP SCIENCE                                        Non
          Digestion & Evaporation Systems              Reactive
                                                       Samples
Method Development Guide
Non Reactive samPLES

              NON REACTIVE EXAMPLES
              i.e. Drinking Water, Waste Water

                    Sample, (Hg analysis) -
                   Water/Soil

                                                Choose Acid Combination

PlasmaPURE HCl Acid                             PlasmaPURE HNO3 Acid                                      PlasmaPURE HNO3/HCl Acids
- Strong non-oxidizing mineral acid             - Strong oxidizing mineral acid                           - Very strong oxidizing media
                                                - Sample digested between 65°C and 95°C                   - Reacts upon mixing - forms brown fumes upon mixing
- Sample should be between 65°C                 - DigiTUBEs, Watch Glasses                                - Samples should be digested between 65°C and 95°C
                                                                                                          - DigiTUBE, Glass, or Quartz sample tubes, Watch
  and 95°C
- DigiTUBE, Glass, or Quartz sample                                                                         Glasses

  tubes, Watch Glasses

                                                   System Used: DigiPREP MS*, DigiPREP LS*,
                                                   DigiPREP Jr.*, DigiPREP h and DigiPREP MINI

                                                * Used with KeyPad, PC Classic or Touch Screen controller

                                                SOLID                                                     LIQUID  *Suggestion for Hg in Water Only*
                                                                                                                  To prevent pressure build-up, loosen

                                                                                                                              the cap by 1/4 turn.

2 grams of solid sample                                                                                   - 50 ml of liquid sample
  - max 10 ml acid                                                                                        - Can use closed caps *

                                 Digest Sample                                                                          Digest and Concentrate

                                                                                           Filter Sample                   DigiSET
                                                                                          (if necessary)          - used for unattended

                                                                                 Digestion                              evaporation
                                                                                 Complete
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